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Hydrogenation with an H₂ balloon template

Hydrogenation with an H₂ balloon template: Stirred flask of substrate and Pd/C in solvent, sealed with a septum; H₂ balloon on a needle, with a vent needle for purging. University.
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Stirred flask of substrate and Pd/C in solvent, sealed with a septum; H₂ balloon on a needle, with a vent needle for purging. University.

What the template shows

  • Reduce C=C (or remove a benzyl group) with H₂ gas over a palladium on carbon catalyst
  • Vent needle
  • For the purge only: flush the flask with N₂, then let H₂ from the balloon sweep out through it; then remove it
  • Tight fit; a slight positive H₂ pressure
  • Add the catalyst first under N₂, then the solvent (EtOH, MeOH or EtOAc); dry Pd/C can ignite solvent vapour
  • Stir fast
  • Gas, liquid and solid must mix; no heating
  • Double balloon on a needle (about 1 atm); refill it when it shrinks. A Parr shaker is used for higher pressures. H₂ is flammable: fume hood, no flames
  • Purge with N₂, filter through Celite, keep the filter cake wet with water (it can ignite when dry)
  • Reaction setup

Drawn with 15 shapes – every one editable in MolDraw.

Sources

How to use this template

  1. Press Edit in MolDraw. The template opens on the canvas of the free MolDraw editor.
  2. Change anything: move structures, edit atoms and labels, recolour highlights or delete what you do not need.
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Frequently asked questions

Is the Hydrogenation with an H₂ balloon template free?

You can preview the Hydrogenation with an H₂ balloon template here and open and edit it in MolDraw for free. Downloading or exporting it is part of MolDraw Pro, together with the other premium templates.

Can I edit the Hydrogenation with an H₂ balloon template?

Yes. It opens as an ordinary MolDraw drawing, so every structure, arrow, label and colour can be changed, and you can add your own content around it.

Is the chemistry checked?

Every structure is checked with RDKit and every curly arrow passes MolDraw’s electron-flow audit. The sources used are listed on this page.

Can I edit the glassware?

Yes. Every piece of glassware is a MolDraw apparatus object: move, resize, recolour the liquid or swap a piece and the joints stay connected.

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